Calibration of gas analysis devices with open cuvette
| Назва | Calibration of gas analysis devices with open cuvette |
| Назва англійською | Calibration of gas analysis devices with open cuvette |
| Автори | Yurii Bilak, Volodymir Kozubovsky, Marianna Rol |
| Принадлежність | Uzhhorod National University, Uzhhorod, Ukraine |
| Бібліографічний опис | Calibration of gas analysis devices with open cuvette / Yurii Bilak, Volodymir Kozubovsky, Marianna Rol // Scientific Journal of TNTU. — Tern.: TNTU, 2024. — Vol 114. — No 2. — P. 135–140. |
| Bibliographic description: | Bilak Y., Kozubovsky V., Rol M. (2024) Calibration of gas analysis devices with open cuvette. Scientific Journal of TNTU (Tern.), vol 114, no 2, pp. 135–140. |
| DOI: | https://doi.org/10.33108/visnyk_tntu2024.02.135 |
| УДК | 543.544.5:543.42 |
| Ключові слова | gas analyzer, calibration, radiation, calibration interval, open cuvette. |
Gas analysis devices are measuring instruments and require periodic confirmation of their metrological parameters. This paper deals with methods of metrological support of measurements of absorption remote devices (with open cuvette). The design of the device where the operating and calibration cuvettes (with calibration gas mixture) are alternately (if necessary) placed on the optical path of the device, with the same optical elements. is proposed. This method of calibration and verification allows you to do without the use of CGM, which greatly simplifies calibration and verification of the gas analyzer at the workplace. In addition, the method reduces the calibration and verification error, since in the calibration mode the light flux passes along the same optical path as in the measurement mode, while the light flux and the degree of contamination of the optical elements by selective and non-selective components of the analyzed mixture remain unchanged. | |
| ISSN: | 2522-4433 |
| Перелік літератури |
1. Pavkhan T. I., Kozubovsky V. R. AC. No.1549314. USSR MKI G 01 N 21/61. The modulator of a single-beam multichannel analyzer. Declared 14.12.87, For administrative use, 4 pp., 1 liter. il.
2. Kozubovsky V. R., Povhan T. I. AC. No. 1559878. USSR MKI G 01 N 21/61. The method of calibration of the gas analyzer. Declared 6.06.88, For administrative use, 4 pp., 1 liter. il.
3. Kozubovsky V. R., Povhan T. I. AC. No. 1598652. USSR MKI 01 N 21/61. One-beam multichannel analyzer. Declared 23.03.89, For administrative use, 4 pp., 1 liter. il.
4. Kozubovskyi V. R. The method of calibration and verification of the gas analyzer. Metrology and devices, 2011, no. 4, pp. 41–43.
5. Kozubovsky V. R., Bilak Yu. Yu. Express analysis of gas mixtures using a spectral correlator based on the fabry–perot interferometer. Journal of Applied Spectroscopy, 2022, vol. 89, no. 3, pp. 495–499.
6. Kozubovskyi V. R., Bilak Yu. Yu. Method of calibration and verification of a gas analyzer with an open cuvette (trace). XXII International scientific and technical conference “Device construction: status and prospects”, 2023, May 16–17, KPI named after Igor Sikorskyi, Kyiv, Ukraine.
7. Kozubovsky V. R., Bilak Y. Yu., Rol M. I. Calibration of gas analysis instruments. XXII International Scientific and Technical Conference “Instrument Construction: Status and Prospects”, 2023, May 16–17, KPI named after Igor Sikorskyi, Kyiv, Ukraine.
8. O'Keeffe A. E., Ortman G. C. Primary Standards for Trace Gas Analysis. Anal. Chem.1966, 38, 6, pp. 760–763.
9. Udina S., Carmona M., Pardo A. et al. A micromachined thermoelectric sensor for natural gas analysis: Multivariate calibration results Sensors and Actuators B: Chemical, 2012, vol. 166–167, pp. 338–348.
10. Baskin Z. L. Dynamic methods for calibration and verification of the metrological characteristics of instruments intended for gas analysis (generalized approach), 2008, Inorg Mater, vol. 44, pp. 1606–1611.
11. Pevzner E. A., Kalinnikova N. D. Device for calibration of gas analyzers. Device for calibration of gas analyzers NASA Transl. into ENGLISH from Prib. Sist. Upr. 1974, USSR 2, pp. 40–41.
12. Available at: https://zakon.rada.gov.ua/rada/show/v0118774-23#Text
13. Perehud E. A., Gorelyk D. O. Measuring methods of atmospheric pollution control, 1981, Khimiya, 383 p.
14. Kozubovsky V. R. Method for calibration and calibration of gas analyzer. Utility Model Patent, no. 461127, Published July 11, 2011 Bul. № 13. |
| References: |
1. Pavkhan T. I., Kozubovsky V. R. AC. No.1549314. USSR MKI G 01 N 21/61. The modulator of a single-beam multichannel analyzer. Declared 14.12.87, For administrative use, 4 pp., 1 liter. il.
2. Kozubovsky V. R., Povhan T. I. AC. No. 1559878. USSR MKI G 01 N 21/61. The method of calibration of the gas analyzer. Declared 6.06.88, For administrative use, 4 pp., 1 liter. il.
3. Kozubovsky V. R., Povhan T. I. AC. No. 1598652. USSR MKI 01 N 21/61. One-beam multichannel analyzer. Declared 23.03.89, For administrative use, 4 pp., 1 liter. il.
4. Kozubovskyi V. R. The method of calibration and verification of the gas analyzer. Metrology and devices, 2011, no. 4, pp. 41–43.
5. Kozubovsky V. R., Bilak Yu. Yu. Express analysis of gas mixtures using a spectral correlator based on the fabry–perot interferometer. Journal of Applied Spectroscopy, 2022, vol. 89, no. 3, pp. 495–499.
6. Kozubovskyi V. R., Bilak Yu. Yu. Method of calibration and verification of a gas analyzer with an open cuvette (trace). XXII International scientific and technical conference “Device construction: status and prospects”, 2023, May 16–17, KPI named after Igor Sikorskyi, Kyiv, Ukraine.
7. Kozubovsky V. R., Bilak Y. Yu., Rol M. I. Calibration of gas analysis instruments. XXII International Scientific and Technical Conference “Instrument Construction: Status and Prospects”, 2023, May 16–17, KPI named after Igor Sikorskyi, Kyiv, Ukraine.
8. O'Keeffe A. E., Ortman G. C. Primary Standards for Trace Gas Analysis. Anal. Chem.1966, 38, 6, pp. 760–763.
9. Udina S., Carmona M., Pardo A. et al. A micromachined thermoelectric sensor for natural gas analysis: Multivariate calibration results Sensors and Actuators B: Chemical, 2012, vol. 166–167, pp. 338–348.
10. Baskin Z. L. Dynamic methods for calibration and verification of the metrological characteristics of instruments intended for gas analysis (generalized approach), 2008, Inorg Mater, vol. 44, pp. 1606–1611.
11. Pevzner E. A., Kalinnikova N. D. Device for calibration of gas analyzers. Device for calibration of gas analyzers NASA Transl. into ENGLISH from Prib. Sist. Upr. 1974, USSR 2, pp. 40–41.
12. Available at: https://zakon.rada.gov.ua/rada/show/v0118774-23#Text
13. Perehud E. A., Gorelyk D. O. Measuring methods of atmospheric pollution control, 1981, Khimiya, 383 p.
14. Kozubovsky V. R. Method for calibration and calibration of gas analyzer. Utility Model Patent, no. 461127, Published July 11, 2011 Bul. № 13. |
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